AbstractThe purpose of this work was to study the physical and chemical stability of the mango peel powder produced by hot-air drying. Sorption isotherms at 25 °C and glass transition temperatures (T_g) of the samples in equilibrium at different a_w were determined. The degradation of vitamin C and color parameter b* was evaluated along storage under controlled conditions (relative humidity = 60%, temperature = 10, 25 and 35 °C) during 180 days. GAB model well-described water adsorption of the product, showing a monolayer moisture content (X_m) of 0.1260 g water/g dry solids and a critical a_w of 0.56. The Gordon-Taylor model predicted the plasticizing effect of water on glass transition temperature, since T_g of the powders kept at different relative humidity conditions decreased as water activity increased. No visual signs of agglomeration and darkening were observed for samples stored at a_w ≤ 0.529. The powders are a source of calcium and rich in potassium, copper, magnesium and manganese. The concentration of inorganic contaminants and pesticide residues were below the maximum allowed limits. The degradation of vitamin C and color parameter b* followed the first and zero-order kinetic models, respectively. The study indicated good stability for the powders along the storage at 10 and 25 °C, which can be incorporated into different food products, showing high retention of vitamin C, phenolic compounds, antioxidant activity and maintenance of color characteristics.