Published in

International Union of Crystallography, Journal of Applied Crystallography, 4(51), p. 1226-1228, 2018

DOI: 10.1107/s1600576718009147

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Angle calculations using two detector circles and wavelength

Journal article published in 2018 by Hoydoo You ORCID
This paper was not found in any repository, but could be made available legally by the author.
This paper was not found in any repository, but could be made available legally by the author.

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Abstract

A `2D + λ' mode using two detector angles and wavelength is added to the modes of operation of a six-circle diffractometer, i.e. `4S + 2D' diffractometer [You (1999). J. Appl. Cryst. 32, 614–623]. In synchrotron sources, the X-ray energy, and hence the wavelength, can be a degree of freedom for angle calculations. For diffractometers with two detector circles, therefore, the variable X-ray energy can be the third degree of freedom, sufficient for accessing reciprocal space without rotating the sample. This mode is useful for limited sample rotations or X-ray beams focused smaller than the diffractometer circle of confusion.