Metal ceramics are a important new engineering materials with the advantages of ceramics and metal materials. The Al-Al₂O₃ metal ceramics were prepared via the powder metallurgy methods and characterized in this paper, which lay the base for preparing the high performance cermet materials. Through the results and analysis, the conclusions are shown that the relative density is increased with a increasing forming pressure, the electrical resistivity is decreased with a increasing forming pressure. The relative density is increased with a increasing sintering temperature under 700°C, the relative density decreases with a increasing sintering temperature above 700°C, the electrical resistivity is shown the opposite tendency. Through the optimizing the technological parameter, such as the sintering temperature at 700°C, the forming pressure under 20MPa, the Al content for 75wt%, Al-Al₂O₃ metal ceramics are successfully prepared with the high relative density and the low electrical resistivity, the relative density is 97.52%, and the electrical resistivity is 101.34Ω·m