Published in
Springer Verlag, Chemistry of Natural Compounds, 2(40), p. 134-136
DOI: 10.1023/b:conc.0000033928.00722.fa
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Formation of the Dinitro-3H-pyrazole Derivative of Cycloartemisiaketone Oxime
Journal article published in 2 by
E. M. Suleimenov,
Raldugin Va,
I. Yu,
Atazhanova Ga,
G. A. Atazhanova,
A. T. Kulyyasov,
V. A. Raldugin,
I. Y.-U. Bagryanskaya,
Y.-U. V. Gatilov,
M. M. Shakirov,
S. M. Adekenov
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Abstract
3aR * ,6aR *)-3,3,5,5-Tetramethyl-3a,6a-dinitro-3a,6a-dihydro-3H-cyclopentano[c]pyrazol-2-oxide was formed by reaction of cycloartemisiaketone oxime [4,4-dimethyl-2-(1-methylethylidene)cyclopentanone oxime] with AcOH and NaNO 2 in CHCl 3 solution. The structure was solved by x-ray structure analysis.