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Published in

International Union of Crystallography, Journal of Applied Crystallography, 4(44), p. 763-771, 2011

DOI: 10.1107/s0021889811016232

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Low-energy contamination of Mo microsource X-ray radiation: analysis and solution of the problem

Journal article published in 2011 by Piero Macchi ORCID, Hans-Beat Bürgi, Abita S. Chimpri, Jürg Hauser, Zoltán Gál
This paper was not found in any repository, but could be made available legally by the author.
This paper was not found in any repository, but could be made available legally by the author.

Full text: Unavailable

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Data provided by SHERPA/RoMEO

Abstract

In recent years, microsource sealed tubes in combination with multilayer optics have been adopted in many crystallography laboratories for very low power X-ray generation, monochromatization and high-brilliance microfocusing. All these factors allow high-performance experiments on a laboratory scale. However, a fundamental defect of this technology has been discovered, namely a significant contamination of the characteristic radiation by low-energy photons. Some simple experiments are reported, showing that the contamination can significantly reduce the accuracy of the measured intensities, especially when Mo Kα radiation is used. A simple and economic solution to the problem is proposed: an aluminium filter approximately 100 µm thick, which efficiently removes the low-energy contaminant photons.