International Union of Crystallography, Journal of Applied Crystallography, 4(44), p. 763-771, 2011
DOI: 10.1107/s0021889811016232
Full text: Unavailable
In recent years, microsource sealed tubes in combination with multilayer optics have been adopted in many crystallography laboratories for very low power X-ray generation, monochromatization and high-brilliance microfocusing. All these factors allow high-performance experiments on a laboratory scale. However, a fundamental defect of this technology has been discovered, namely a significant contamination of the characteristic radiation by low-energy photons. Some simple experiments are reported, showing that the contamination can significantly reduce the accuracy of the measured intensities, especially when Mo Kα radiation is used. A simple and economic solution to the problem is proposed: an aluminium filter approximately 100 µm thick, which efficiently removes the low-energy contaminant photons.