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Royal Society of Chemistry, Analytical Methods, 20(5), p. 5386

DOI: 10.1039/c3ay41136b

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Expedient preparative isolation, quantification and characterization of limonoids from Neem fruits

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This paper is available in a repository.

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Abstract

Major basic limonoids from Neem fruits such as azadirone, epoxyazadiradione and azadiradione were isolated in preparative scale using an automated and rapid medium pressure liquid chromatography (MPLC)-based protocol. They were individually quantified using HPLC. An LC-ESI-MS/MS-based rapid identification technique was developed for the high-throughput screening of these limonoids in phytochemical extracts.