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Royal Society of Chemistry, CrystEngComm, 10(12), p. 2826

DOI: 10.1039/b922687g

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Solid-state 51V MAS NMR spectroscopy determines component concentration and crystal phase in co-crystallised mixtures of vanadium complexes

Journal article published in 2010 by Ulla Gro Nielsen ORCID, Alan Hazell, Jørgen Skibsted, Hans J. Jakobsen, Christine J. McKenzie
This paper was not found in any repository, but could be made available legally by the author.
This paper was not found in any repository, but could be made available legally by the author.

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Abstract

The oxo-peroxo-vanadium(v) and dioxo-vanadium(v) complexes of N,N-bis(2-pyridylmethyl)glycinate (bpg(-)), VO(O-2)(bpg) (1) and V(O)(2)(bpg) (2) co-crystallize in variable ratios in an anhydrous and a dihydrate phase with the overall formulation 1(x)2(1-x)center dot nH(2)O, n = 0 or 2, where 0