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American Institute of Physics, Review of Scientific Instruments, 7(93), 2022

DOI: 10.1063/5.0098893

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Operando reaction cell for high energy surface sensitive x-ray diffraction and reflectometry

Journal article published in 2022 by R. Gleißner ORCID, E. E. Beck ORCID, Simon Chung ORCID, G. D. L. Semione ORCID, N. Mukharamova ORCID, G. Gizer ORCID, C. Pistidda ORCID, D. Renner, H. Noei ORCID, V. Vonk ORCID, A. Stierle ORCID
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This paper was not found in any repository, but could be made available legally by the author.

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Abstract

A proof of concept is shown for the design of a high pressure heterogeneous catalysis reaction cell suitable for surface sensitive x-ray diffraction and x-ray reflectometry over planar samples using high energy synchrotron radiation in combination with mass spectrometry. This design enables measurements in a pressure range from several tens to hundreds of bars for surface investigations under realistic industrial conditions in heterogeneous catalysis or gaseous corrosion studies.